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71.
In recent years, porous silicon (PSi) has attracted a great deal of attention for sensing applications. However, the high reactivity of PSi surfaces causes serious problems of stability. In this work, we developed new thin films that can serve as stabilizer of PSi for CO2 gas sensors development. PSi surface was coated with carbon nitride (CNx) film which is one of the most important interfering to stabilize the PSi layer. CNx film was deposited by pulsed laser ablation. The effect of CO2 gas on the sensor response was investigated for different polarization voltages. The electrical properties of (Al/CNx/PSi/Si) structure were modified in the presence of the gas. The device shows a high sensitivity against CO2 gas. Furthermore, the current variation of the sensor as a function of time has been investigated. The results show that the Al/CNx/PSi/Si structure becomes stable after the first two weeks. 相似文献
72.
In this paper, we propose a new angle quantization index modulation (AQIM) method, called the difference AQIM (DAQIM) method. The proposed method aims to improve the watermarking performance against gain attacks. Unlike the original AQIM method (Ourique et al., Angle QIM: a novel watermark embedding scheme robust against amplitude scaling distortions, in: Proceedings of IEEE International Conference on Acoustics, Speech, and Signal Processing, vol. 2, 2005, pp. 797–800), the DAQIM method quantizes the difference of the two angles instead of the angles themselves. The main advantage of the DAQIM method is to disperse the interference to the watermark signal from one angle to more angles. Thus, the watermark has a higher ability to resist attacks. We perform a theoretical analysis of the document-to-watermark ratio (DWR) based on our proposed method. We show that our proposed method can obtain a lower embedding distortion compared to the AQIM and the gradient direction watermarking (GDWM) (Nezhadarya et al., IEEE Trans. Inf. Forensics Secur., 6(4), 2011, 1200–1213), methods under the same robustness and payload conditions. The experimental results demonstrate that our proposed method outperforms common existing methods in terms of the robustness against various attacks such as the JPEG quantization noise, additive white Gaussian noise (AWGN), cropping effect and mean filtering. 相似文献
73.
The layer-by-layer (LBL) polyelectrolyte deposited membranes have drawn increasing attention in various applications due to the ease of selective layer formation and their stability and versatility. In this study, the LBL deposition was performed at the inner surface of the polyethersulfone (PES) hollow fiber substrate to form composite nanofiltration (NF) membrane. The semi-dynamic deposition procedure was adopted with the aid of syringes. The newly developed inner deposited (id-LBL) membranes were then tested in NF and forward osmosis (FO) applications and the performance were compared with outer surface deposition as well as some literature data. The id-LBL membranes could not only withstand higher operating pressure but also possess superior hardness rejection especially in high concentration mixed salt solutions (more than 95% rejection to Mg2+ and Ca2+ in a 5000 ppm total dissolved salt (TDS) mixture under 4.8 bar). As for the FO process, with only two layer deposition, the id-LBL membranes also demonstrated significant performance improvement with increased water flux (up to 70 L/m2 h using 0.5 M MgCl2 as draw solution in active layer facing draw solution configuration) and reduced salt leakage (around 0.5 g/m2 h using 1 M MgCl2 draw solution in active layer facing feed water configuration). This study suggests that for hollow fiber substrate, the inner surface is more suitable for the formation of the selective layer via LBL deposition than the outer surface. 相似文献
74.
Three various 12CrNi2 alloy steels were successfully fabricated on 35CrMo alloy steel by laser melting deposition with the aim of investigating the effect of powder oxygen content on formability of 12CrNi2 alloy steel. The phase constituents, macroscopic morphology, microstructure, and microhardness of powders and samples were studied by some modern analysis methods. The experimental results showed that with the increase of the oxygen content from 220 to 600?ppm, the sphericity and density of the powders gradually decreased which led to the appearance of pores in the as-deposited samples. The phase constituent of three as-deposited samples with different oxygen contents was α-Fe(M) phase. The percentage porosity in the macroscopic morphology increased with the increase of the oxygen content. Meanwhile, the high oxygen content contributed to more pores and the crack formation in the microstructure. With the increase of oxygen content, the microhardness of the as-deposited samples would decrease. 相似文献
75.
Wei Shao Qianqian Pan Qiaoli Chen Chongzhi Zhu Weijian Tao Haiming Zhu Huijun Song Xuelu Liu Ping-Heng Tan Guan Sheng Tulai Sun Xiaonian Li Yihan Zhu 《Advanced functional materials》2021,31(3):2006738
Metallic nanocrystals manifest themselves as fascinating light absorbers for applications in plasmon-enhanced photocatalysis and solar energy harvesting. The essential challenges lie in harvesting the full-spectrum solar light and harnessing the plasmon-induced hot carriers at the metal–acceptor interface. To this end, a cooperative overpotential and underpotential deposition strategy is proposed to mitigate both the challenges. Specifically, by utilizing both ionic additive and thiol passivator to introduce symmetry-breaking growth over gold icosahedral nanocrystals, the microscopic origin can be attributed to the site-specific nucleation of stacking faults and dislocations. By adopting asymmetric crystal shape and unique surface facets, such nanocrystals attain high activity toward photocatalytic ammonia borane hydrolysis, arising from combined broadband plasmonic properties and enhanced direct transfer of hot electrons across the metal–adsorbate interface. 相似文献
76.
Dams disrupt the flow of water and sediment and thus have the potential to affect the downstream geomorphic characteristics of a river. Though there are some well‐known and common geomorphic responses to dams, such as bed armouring, the response downstream from any particular dam is dependent on local conditions. Herein, we investigate the response of the upper Santa Ana River in southern California, USA, to the construction of a large dam at the transition from mountains to valley, using calculations of bedload transport capacity on the mainstem below the dam and for major tributaries. Approximate sediment budgets were constructed for downstream reaches to estimate deposition and erosion rates for sand, gravel, and cobble particle sizes. Our results indicate that the classical response of bed armouring and erosion is likely limited to a short reach immediately below the dam. Farther downstream, though transport capacity is reduced by flow regulation by the dam, the channel reaches are likely to remain depositional but with reduced deposition rates. Persistent deposition, as opposed to erosion, is the result of the replenishment of flow and sediment supply by large downstream tributaries. In addition, the calculations indicate that the composition of the bed is unlikely to change substantially in downstream reaches. A Monte Carlo approach was employed to estimate the uncertainty in the sediment budget predictions. The impacts of the dam on the geomorphic character of the river downstream could have implications for native fish that rely on coarse substrate that supports their food base. 相似文献
77.
78.
设计开发一种具有高通量、低流阻特征的空心锥喷嘴,并通过理论与实验方法研究空心锥喷嘴的喷淋性能,基于准自由涡理论建立空心锥喷嘴内部流体流动的数学模型,阐明流量系数、喷淋锥角、喷嘴流量与喷嘴结构参数之间的定量关系,并利用多效蒸馏海水淡化喷淋实验台对理论计算结果进行实验测试和验证。研究结果表明:正常工作状态下喷嘴流量系数、喷淋锥角、喷淋流量等参数理论值与测量值之间的误差小于5%,验证了设计模型的准确性。同时根据实验测试数据,拟合得到该类型空心锥喷嘴喷淋锥角与雷诺数之间的经验公式,可为蒸馏海水淡化用大流量空心锥喷嘴的结构设计、工艺选型提供理论指导和数据支持。 相似文献
79.
《Journal of the European Ceramic Society》2020,40(10):3577-3584
In this work, the grain boundaries composition of the polycrystalline CaCu3Ti4O12 (CCTO) was investigated. A Focused Ion Beam (FIB)/lift-out technique was used to prepare site-specific thin samples of the grain boundaries interface of CCTO ceramics. Scanning transmission electron microscopy (STEM) coupled with energy dispersive X-ray spectrometry (EDXS) and Electron Energy Loss Spectroscopy (EELS) systems were used to characterize the composition and nanostructure of the grain and grain boundaries region. It is known that during conventional sintering, discontinuous grain growth occurs and a Cu-rich phase appears at grain boundaries. This Cu-rich phase may affect the final dielectric properties of CCTO but its structure and chemical composition remained unknown. For the first time, this high-resolution FIB-TEM-STEM study of CCTO interfacial region highlights the composition of the phases segregated at grain boundaries namely CuO, Cu2O and the metastable phase Cu3TiO4. 相似文献
80.